Catching
the Drift:
What RH Measurement Spec Sheets aren't telling you...
Kevin Bull, Veriteq Instruments
Understanding how humidity measurement devices function and how product
specifications can be misrepresented can mean the difference between
purchasing an expensive system with inherent measurement flaws and
getting a system that measures accurately between calibrations.
The ability to scrutinize
product specs in greater depth will allow you to select a system that fits the measurement needs of your application. This, in turn can help with meeting compliancy and quality assurance requirements.
Far too often, RH product
specifications not listed on a data sheet can be more
revealing than those that are...
Measuring Humidity: How hard can it be?
One of the hardest parameters to accurately measure, relative humidity is a
critical factor across a broad spectrum of industries. Moreover, humidity has
the potential to impact critical applications in ways that are often hard to
detect until something goes catastrophically wrong.
In calibration, stability
testing, and quality assurance processes, the uncertainty of humidity
measurement can be a major source of unnecessary cost, skewed data, and
lost revenues.
The Inevitable Drift of Humidity Sensors
It’s an immutable law of metrology: all sensors drift. Humidity sensors are uniquely prone to drift however, for the simple reason that they’re “air breathers.” Unlike temperature sensors, humidity sensors must be in direct contact with the environment.
Not only is
the air constantly changing temperature, (which affects RH) but also contains countless contaminants
that affect the sensor. Unlike temperature sensors, the internal structure of
the RH sensor is has no protective barrier from airborne elements, so the
sensor’s ability to measure degrades over time.
This is why, even if the calibration process were perfect (it isn’t), once
exposed to the real world, the measurement accuracy decreases
until the next time the device is calibrated. However, between setting up a
recently calibrated RH sensor and recalibration, what critical processes and
products are have been affected?
A Tale of Two Accuracies (Initial vs. One Year Later)
When looking at any RH measuring device’s product specifications, there are two key accuracy values that must be considered. The first is initial accuracy, or, the accuracy of the device when first deployed; the other value is one-year
accuracy or the accuracy of the device when you go to recalibrate it (6
months to 1 year after deployment).
However, it is important to note that
not all initial accuracies are created equal; to be complete, initial accuracy
must factor in all known uncertainties. This is where product specifications can differ greatly from sensor to sensor.
In an ideal world, RH system data sheets would include each of the following sources of
error:
• Calibration Uncertainty
• Temperature Effect & Mathematical Fit
• Hysteresis
• Measurement Resolution
If these variables can’t be found on you product’s specifications, you cannot
be certain that they have been included in calculating that device’s accuracy.
What to Look for in Humidity Product Specs
Accuracy One Year Later...
(How long have you been OOS and by how much?)
Although a critical value, one-year accuracy is rarely included on product
specifications for humidity measuring instruments. However, this percentage
is actually more important than initial accuracy because all data gathered
since the last calibration is based solely on its accuracy upon re-calibration.
If your RH device is found Out-Of-Spec when you go to re-calibrate, you will
be faced with some hard questions. What products or tests were affected and
to what extent?
You may be able to find specs on the accuracy of an RH measuring device
after a year of typical use and over a wide temperature range, but first you’ll
have to know what to look for and secondly, you’ll have to look at a lot of
product spec sheets.
If there are no values listed for a device at the end of its calibration interval, you may have to just ask the sales representative.
However, this comes with a proviso; the manufacturer should provide
documentation that shows the accuracy values of their devices at the end of
the calibration cycle, before re-calibrating.
But, the question remains: why is the inclusion of these values on product specifications
so rare?
The Elements of Error:
To understand accuracy values and their inclusion or exclusion from spec sheets, it’s vital to understand three major determinants of sensor accuracy:
• Sensor characteristics
• Calibration
• Sensor Measurement System (Electronics)
A device may have the best RH sensor available; however, as already stated,
all RH sensors drift. To maximize overall accuracy, it is crucial to reduce
errors that occur during the calibration process and within the entire sensor
measurement system. When these elements are well controlled, it creates a bit of
"head room" for the inexorable drift of the device.
In other words, to anticipate the drift of a device, optimal accuracy must be obtained at the calibration stage; with calibration being performed in a way that virtually eliminates all other sources of error.
Sources of Error & Their Impact
Calibration Uncertainty
All humidity calibration chambers have an associated uncertainty, a major
source of which is temperature non-uniformity, which must be factored into a
measuring device’s accuracy specification.
In the case of RH sensor equipped
data recorders, the manufacturers must perform a high-accuracy temperature
calibration. Each recorder’s measured temperature is then able to
compensate for chamber non-uniformity during RH calibration — greatly
reducing this source of error.
Interestingly, the location of the temperature and RH sensors inside a data
recorder can actually have an effect on the accuracy of the calibration. Inside the best available data recording devices you will find temperature sensor is placed right beside the RH sensor. Proximity allows both sensors to read the same environment, eliminating any discrepancies (however small) between their measurements.
Temperature Effect & Mathematical Fit
Most RH measuring devices are calibrated to measure at one specific
temperature (typically 25ºC). But, unless the device will only measure humidity at that temperature, there can be significant temperature-related inaccuracies.
To solve this, a manufacturer can include tables that correlate humidity
measurement over a wide range of calibrated temperatures in the memory of
the device. Ideally, no two data recorders have the same set of tables
because each set is calibrated to the unique components of every recorder. View sample table.
This creates a more intelligent device because the tables contain explicit
information on how to measure humidity over a wide temperature range. This
kind of device-specific calibration is critical in the case of ICH (stability) applications due to the range of environments and accuracy required for compliance.
Hysteresis
Hysteresis is the tendency of measuring devices to not return completely to
their original state after a change has been measured. It’s also a major
source of error. Unfortunately, despite its ubiquity, too few data sheets
include hysteresis as a factor in their accuracy values.
Unfortunately, if hysteresis appears at all, it’s
often de-emphasized by being placed far apart from the total accuracy
specification. Hysteresis unmentioned or disconnected textually from an
accuracy value could be considered product misrepresentation to a discerning
purchaser.
Measurement Resolution & Electronics
Resolution is simply the smallest measurable increment that the device can
detect. A good device will feature a 12-bit high-resolution system that detects
changes of as small as 0.05%RH.
A very significant element that affects a device’s accuracy is its electronic components. Electronics systems are greatly impacted by temperature, which
in turn affects overall accuracy. One challenge that manufacturers face is
trying to get the electronic system to remain stable over wide temperature
ranges.
As an example, Veriteq Instruments, a manufacturer of high-end industrial
Temp/RH measurement systems, found that a synchronous bridge
measurement system features low power and superior stability. This unique
combination greatly reduced the electronics-associated error in humidity measurement.
For a more in-depth discussion of bridge measurement systems, please
see: "Methods
of Accurately Measuring Capacitive RH Sensors" originally presented
at the Worldwide Humidity Symposium in 2006.
Conclusion: Catching the Drift means Getting the Numbers
Product specifications, often one of the key pieces of information used by decision
makers in selecting measurement systems, must be explicit, easy-to-understand, and straightforward.
An explicit listing of all known influences and sources
of error — calibration uncertainty, temperature effect, measurement
resolution, and hysteresis — should be included in the accuracy value stated
on any data sheet.
If these values are not mentioned in product specs the consumer is
left to ask: have they been included in that product’s stated accuracy?
Until
those who equip laboratories are better informed on all factors that
contribute to inaccuracy in humidity measuring devices, manufacturers
confronted with their own out-of-spec devices upon re-calibration, can always
blame drift.
1. Methods
of Accurately Measuring Capacitive RH Sensors by Kevin Bull, presented
at 5th International Symposium on Humidity & Moisture; ISHM 2006,
Rio de Janeiro, Brazil.
2. To see a sample of “Initial Accuracy” and “One
Year Accuracy” specifications, see VL
2000 data loggers Spec Sheet.
About Kevin Bull...
For further information, please contact: customersupport@veriteq.com
About Veriteq
From pharmaceutical and biotech, calibration laboratories, aerospace engineering facilities, to storage facilities for sensitive products, Veriteq provides monitoring, alarming, and validation systems for controlled environments.
With the only system to offer gap-free data in the event of power or network failures — Veriteq provides a fail-safe solution wherever the consequences of lost or inaccurate data are serious.
For more information call 800 683 8374 (or 604 273 6850), contact us online, or email a Veriteq representative.
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